TA Instruments

Papa china-0024f

27/04/2022 11:32:35 a. m.

Sample name	Papa china
Sample notes	 
Experiment notes	
Operator	
Sample density	1,000 g/cm^3
Results file name	Papa china
Run number	24 
Results directory	C:\Ta\Data\Ar1500\Ar1500\DIEGO ROA
Experiment was run on	27/04/2022 11:32:35 a. m.

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 1
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 2
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 3
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 4
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Conditioning Step 2
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	10,00 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Temperature ramp step 1
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	25,0 C
End temperature	90,0 C
Wait for start temperature	Yes
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 2
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	90,0 C
Wait for start temperature	No
Ramp duration	0:05:00 hh:mm:ss
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 3
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	25,0 C
Wait for start temperature	No
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Conditioning Step 3
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	1,000 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 5
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 6
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 7
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 8
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	No
Set temperature system idle	No

Geometry name	Starch cell
Geometry notes	Starch cell
Geometry material	High temperature
gap	5500 micro m
Calibration factor	10800 
Gap offset	0 micro m
Geometry inertia	2,236 micro N.m.s^2
Shear rate factor	1,000 
Shear stress factor	10800 1/m^3
Measurement system factor	10800 1/m^3
Fluid density factor	1,000E-15 m^5
Normal force factor	1,000 1/m^2
Backoff distance	1,25E5 micro m

Gap zero mode	Standard
Sample compression	none 
Compression distance	1000,0 micro m
Compression velocity	100,0 micro m/s
Fine velocity	1000,0 micro m/s
Coarse velocity	3000,0 micro m/s
Other velocity	3000,0 micro m/s
Current temperature system	Starch cell
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	5,0 C
Cooling water range	15,0 C
Bearing friction correction	Yes
Bearing friction	1,222 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1,0000 , offset 0 C
	Water bath - span 1,0000 , offset 0 C
	Torsion oven - plate - span 1,0000 , offset 0 C
	Torsion oven - solid sample - span 1,0000 , offset 0 C
	Peltier concentric cylinders - span 1,0000 , offset 0 C
	None - span 1,0000 , offset 0 C
	Stress relaxation - span 1,0000 , offset 0 C
	Current temperature system - span 1,0000 , offset 0 C
Bearing mapping type	fast 
Number of mapping iterations	1
Instrument type (MType)	AR1500ex
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	172.23.191.2
Software version	V5.8.2
Windows version	Windows XP 6.2
Instrument inertia	15,97 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0,2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0,1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	3,000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	No
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	No
Creep zero displacement	Yes
Store images to the results for creep steps	No
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	No
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	No
Flow torque limit	10,00 micro N.m
Flow velocity limit	1,000E-3 rad/s
Oscillation torque limit	5,00 micro N.m
Oscillation displacement limit	1,00E-5 rad
Oscillation raw phase limit	170,0 degrees
Oscillation minimum normal force limit	0 N
Oscillation maximum normal force limit	0 N
Flow velocity tolerance	5,00 %
Oscillation torque tolerance	1,00 %
Oscillation displacement tolerance	5,00 %
Oscillation velocity tolerance	5,00 %
Temperature tolerance	1,0 C

Stepped flow step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,01328	1,004E-3	13,22	9,9690	25,0	0
0,03152	2,152E-3	14,65	20,000	25,0	0
0,06239	4,640E-3	13,45	30,032	25,0	0
0,1063	9,998E-3	10,63	40,079	25,0	0

Stepped flow step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,1408	9,999E-3	14,09	9,9840	25,0	0
0,1847	0,02154	8,572	20,078	25,0	0
0,2278	0,04641	4,909	30,375	25,0	0
0,2343	0,1000	2,343	40,468	25,0	0
0,2150	0,1000	2,150	50,515	25,0	0

Stepped flow step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,1884	0,1000	1,884	9,9690	25,0	0
0,1512	0,1585	0,9541	20,094	25,0	0
0,1228	0,2512	0,4888	30,188	25,0	0
0,1210	0,3981	0,3039	40,250	25,0	0
0,1217	0,6310	0,1929	50,313	25,0	0
0,1199	1,000	0,1199	60,375	25,0	0

Stepped flow step 4

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,1121	1,000	0,1121	9,9840	25,0	0
0,1112	1,334	0,08338	20,047	25,0	0
0,1084	1,778	0,06094	30,094	25,0	0
0,1086	2,371	0,04581	40,172	25,0	0
0,1054	3,162	0,03332	50,219	25,0	0
0,09172	4,217	0,02175	60,281	25,0	0
0,08805	5,623	0,01566	70,375	25,0	0
0,1114	7,499	0,01486	80,406	25,0	0
0,1725	10,00	0,01725	90,500	25,0	0
0,3088	13,34	0,02316	100,59	25,0	0
0,4650	17,78	0,02615	110,70	25,0	0
0,7138	23,71	0,03010	120,88	25,0	0
1,119	31,62	0,03538	130,95	25,0	0
1,701	42,17	0,04034	140,97	25,0	0
2,831	56,23	0,05035	151,03	25,0	0
4,532	74,99	0,06044	161,16	25,0	0
6,834	100,0	0,06834	171,25	25,0	0

Temperature ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,2105	10,00	0,02105	9,0080	25,0	0
0,2122	10,00	0,02122	18,020	25,5	0
0,2130	10,00	0,02130	27,008	26,6	0
0,2143	10,00	0,02143	35,996	28,0	0
0,2176	10,00	0,02176	45,000	29,7	0
0,2217	10,00	0,02217	54,004	31,5	0
0,2261	10,00	0,02261	63,004	33,2	0
0,2329	10,00	0,02329	72,000	34,9	0
0,2394	10,00	0,02394	81,000	36,6	0
0,2468	10,00	0,02468	90,008	38,2	0
0,2582	10,00	0,02582	98,992	39,8	0
0,2672	10,00	0,02672	108,00	41,3	0
0,2790	10,00	0,02790	117,00	42,8	0
0,2894	10,00	0,02894	126,01	44,4	0
0,2986	10,00	0,02986	135,00	45,9	0
0,3114	10,00	0,03114	144,00	47,4	0
0,3243	10,00	0,03243	153,01	48,8	0
0,3351	10,00	0,03351	161,99	50,3	0
0,3485	10,00	0,03485	171,00	51,8	0
0,3623	10,00	0,03623	179,99	53,3	0
0,3766	10,00	0,03766	189,00	54,8	0
0,3836	10,00	0,03836	198,00	56,3	0
0,3964	10,00	0,03964	207,00	57,9	0
0,4035	10,00	0,04034	216,01	59,3	0
0,4161	10,00	0,04161	225,00	60,8	0
0,4213	10,00	0,04213	234,00	62,3	0
0,4333	10,00	0,04333	243,02	63,8	0
0,4479	10,00	0,04479	252,01	65,3	0
0,4549	10,00	0,04549	261,00	66,8	0
0,4624	10,00	0,04624	270,00	68,2	0
0,4722	10,00	0,04722	279,00	69,7	0
0,4864	10,00	0,04864	288,00	71,3	0
0,5037	10,00	0,05037	297,00	72,9	0
0,5503	10,00	0,05503	306,00	74,5	0
0,7370	10,00	0,07370	315,00	75,9	0
1,539	9,999	0,1539	324,01	77,5	0
3,816	9,999	0,3816	333,00	79,3	0
7,524	9,999	0,7525	342,00	80,8	0
12,79	9,999	1,279	351,00	82,1	0
18,54	10,00	1,854	360,02	83,5	0
23,87	10,00	2,387	369,00	84,8	0

Temperature ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

27,76	9,999	2,777	9,0040	86,5	0
29,78	10,00	2,978	17,992	88,7	0
29,78	10,00	2,978	27,004	90,0	0
29,45	10,00	2,945	35,992	90,6	0
28,25	10,00	2,825	45,000	90,8	0
27,10	10,00	2,710	53,980	90,8	0
26,13	10,00	2,613	62,984	90,8	0
25,26	10,00	2,526	71,988	90,8	0
24,52	9,999	2,452	81,004	90,7	0
23,94	9,999	2,394	89,996	90,6	0
23,35	10,00	2,335	98,988	90,5	0
22,96	10,00	2,296	107,99	90,4	0
22,60	10,00	2,260	116,99	90,3	0
22,31	10,00	2,231	126,00	90,2	0
22,04	9,999	2,205	135,00	90,2	0
21,64	10,00	2,164	143,99	90,1	0
21,38	10,00	2,138	153,01	90,1	0
21,12	10,00	2,112	161,99	90,1	0
20,87	10,00	2,087	171,00	90,1	0
20,63	10,00	2,062	179,98	90,0	0
20,35	10,00	2,035	189,00	90,0	0
20,12	10,00	2,012	198,00	90,0	0
19,94	10,00	1,994	207,00	90,0	0
19,77	10,00	1,977	216,00	90,0	0
19,54	10,00	1,954	224,99	90,0	0
19,31	10,00	1,931	234,00	90,0	0
19,17	10,00	1,917	242,99	90,0	0
18,96	10,00	1,896	252,00	90,0	0
18,78	10,00	1,878	260,99	90,0	0
18,66	10,00	1,866	270,00	90,0	0
18,47	10,00	1,847	279,00	90,0	0

Temperature ramp step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

18,36	10,00	1,836	9,0000	90,0	0
18,25	10,00	1,825	18,008	89,4	0
18,39	10,00	1,839	27,000	86,1	0
18,34	10,00	1,834	36,020	85,3	0
18,39	10,00	1,839	45,004	84,8	0
18,45	10,00	1,845	53,996	83,4	0
18,54	10,00	1,854	62,996	81,4	0
18,66	10,00	1,866	72,000	80,3	0
18,82	10,00	1,882	81,000	78,5	0
18,95	10,00	1,895	90,008	76,8	0
19,11	10,00	1,911	98,992	75,8	0
19,33	10,00	1,933	108,00	73,5	0
19,49	10,00	1,950	116,99	72,4	0
19,78	10,00	1,978	125,99	71,0	0
20,01	10,00	2,001	135,00	68,9	0
20,26	10,00	2,026	144,01	68,3	0
20,65	10,00	2,065	153,00	66,1	0
20,93	10,00	2,093	162,00	64,8	0
21,39	10,00	2,139	171,00	63,6	0
21,89	10,00	2,189	180,00	61,4	0
22,34	10,00	2,234	189,00	60,6	0
22,96	10,00	2,296	198,02	58,6	0
23,45	10,00	2,345	207,00	57,1	0
23,91	10,00	2,391	216,01	56,2	0
24,46	10,00	2,446	225,00	54,0	0
25,02	10,00	2,502	234,00	52,9	0
25,73	10,00	2,573	243,00	51,4	0
26,44	10,00	2,644	252,01	49,6	0
27,23	10,00	2,723	261,00	48,4	0
27,77	10,00	2,777	269,99	46,7	0
28,46	10,00	2,846	279,00	45,2	0
29,03	10,00	2,903	287,99	43,8	0
29,48	10,00	2,948	297,00	42,2	0
30,19	10,00	3,019	306,00	40,8	0
30,92	10,00	3,092	315,00	39,3	0
31,66	10,00	3,166	323,99	37,8	0
32,35	10,00	3,235	332,99	36,3	0
33,10	10,00	3,310	342,00	34,3	0
33,80	10,00	3,380	351,00	33,3	0
34,67	10,00	3,467	359,99	31,9	0
35,60	10,00	3,561	369,00	30,2	0

Stepped flow step 5

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,3032	9,998E-4	303,2	9,9060	25,0	0
0,8053	2,152E-3	374,1	20,063	24,9	0
1,546	4,640E-3	333,2	30,125	25,0	0
2,684	9,998E-3	268,5	40,203	25,0	0

Stepped flow step 6

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

3,276	9,998E-3	327,6	9,9530	25,0	0
4,753	0,02154	220,6	20,031	25,0	0
6,821	0,04642	147,0	30,094	25,0	0
9,296	0,1000	92,96	40,140	25,0	0
9,465	0,1000	94,65	50,219	25,0	0

Stepped flow step 7

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

9,487	0,1000	94,87	9,9530	25,0	0
11,26	0,1585	71,03	20,063	25,0	0
13,21	0,2512	52,60	30,141	25,0	0
15,63	0,3981	39,26	40,219	25,0	0
18,49	0,6309	29,30	50,313	25,0	0
22,02	1,000	22,02	60,422	25,0	0

Stepped flow step 8

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

21,80	1,000	21,80	9,9220	25,0	0
24,80	1,334	18,59	20,032	25,0	0
28,20	1,778	15,86	30,094	25,0	0
31,58	2,371	13,32	40,157	25,0	0
34,62	3,162	10,95	50,266	25,0	0
38,51	4,217	9,131	60,266	25,0	0
42,90	5,623	7,628	70,360	25,0	0
47,63	7,499	6,352	80,360	25,0	0
53,51	10,00	5,351	90,407	25,0	0
60,05	13,34	4,503	100,42	25,0	0
66,52	17,78	3,740	110,50	25,0	0
73,71	23,71	3,108	120,58	25,0	0
81,64	31,62	2,582	130,67	25,0	0
90,54	42,17	2,147	140,78	25,0	0
96,71	56,23	1,720	150,84	25,0	0
107,3	74,99	1,431	160,91	25,0	0
119,4	100,0	1,194	170,99	25,0	0

